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The bulk of the collection contains correspondence and reports concerning Reed's work of the American Home Missionary Society of the Congregational Church in the 1845-1869. Among the topics addressed are slavery and how the church should regard congregations in slave-holding states, founding of churches in Iowa, church finances, and founding a college in Iowa. This is a rich collection for the study of early Congregationalism in Iowa.

Consists mostly of correspondence relating to Mr. Stiles. The material is both business related and personal in nature, including several articles written by Stiles, a series of request and thank you letters for copies of his book, Manual of Public Archives of Iowa, work recommendations, literature relating to the American Historical Association, general correspondence and a paper written by Fleming C. Fraker, Cassius C. Stiles and the Public Archives of Iowa.

Consists mostly of correspondence relating to Mr. Stiles. The material is both business related and personal in nature, including several articles written by Stiles, a series of request and thank you letters for copies of his book, Manual of Public Archives of Iowa, work recommendations, literature relating to the American Historical Association, general correspondence and a paper written by Fleming C. Fraker, Cassius C. Stiles and the Public Archives of Iowa.

The collection contains correspondence between Macy and several people from the 1870s to 1919, including a letter from Woodrow Wilson thanking Macy for a gift and for his congratulations on the 1910 New Jersey gubernatorial election. There are a number of miscellaneous family documents, Macy’s diary from 1864-65 in Savannah, Georgia, and sixty letters of tribute at the time of Macy’s death.

Consists of treasurer's reports, minutes, clippings, and correspondence of the Elizabeth Earle Magoun Club.

Professor Kleinschmidt amassed countless photocopies, copies of microfilm and Sanborn maps, copies of newspaper articles, correspondence, and black and white photographs of local buildings (residences, commercial, college).  In the 1990s, Professor Kleinschmidt expressed his interest in having his collection deposited with the Grinnell College Archives.  Members of the Grinnell Historic Preservation Commission (Lisa Adkins, Don Irving, Cheryl Neubert), conducted interviews with him to access much of his accumulated knowledge about this history of the town, the occupants and the buildings.

Consists of holograph, typescript, and proofs of Joseph Wall's biography, Andrew Carnegie (1970), holograph and typescript of Henry Watterson: Reconstructed Rebel (1956), and of the page proof of Interpreting Twentieth-Century America (1973).  A small part of the collection includes some correspondence connected with Andrew Carnegie. Also included is a typescript of the Grinnell College Faculty Handbook (1969) and talks and memos concerning the Abler-Woodworth controversy of 1974.

The collection is divided into three series: Correspondence & drafts of history; Research materials, notes, etc.; Alumni files arranged chronologically by graduation year.

James McNally collected photographs, both black-and-white and color, that depict buildings and Grinnell scenes from about 1857-1961.  The collection of photographs has been donated to Stewart Library.

Copies of outstanding and representative pictures in the collection were made into slides and the slides donated to the archives.  Vera provided the descriptions of the photographs in 1983.  There are two sets of slides: the original slides and another set that are loaded into a carousel.  The latter set may be borrowed with approval of the College Archivist.

Consists of two diaries written by S. (Sammy) M. Wright of Knoxville, Iowa, during the Civil War. He and his brother William served in Company B, Third Regiment, Iowa Volunteer Infantry.

Mary Gae Wyly graduated from Grinnell College in 1962 and served as a librarian from 1968 to 1976.  This collection contains documents from her desk files, including one on the hiring of blacks and women, and a survey of women on campus for the improvement of Grinnell.

Consists of one letter from I. B. Mc., Mexico, Missouri, to Dr. C. Blish, Hampton, Pennsylvania describing the Iowa Territory.  Written before 1846.

There are two pieces to the Irving Hart collection in the Grinnell College Archives.  One is a letter that Elizabeth Kelsey (Class of 1898) wrote to Hart in April 1898 as he was leaving Grinnell to serve in the Spanish–American War, and the other is an autograph album with signatures of students and faculty from the 1870s when Irving’s mother, Elizabeth Biggar Hart, was a student.

The collection contains letters written to Salter and notes written by Salter. The letters include both personal correspondence and that relating to his affairs: church business, business of Iowa College, Salter’s research into the history of the Dodge family, and a variety of other concerns. One letter of note is from James S. Graham in 1884 who recounts his experience watching President Lincoln while he reviewed the 68th Illinois Infantry Volunteers. Also included is a Saloon Passengers’ List and Track Card from an 1881 voyage on the S.S. Bolivia.